Quality Control of Benzyl Alcohol. Agafonova, AV; Smetanin, IA; Rostovskii, NV; Khlebnikov, AF; Novikov, MS in [Agafonova, Anastasiya, V; Smetanin, Ilia A.; Rostovskii, Nikolai, V; Khlebnikov, Alexander F.; Novikov, Mikhail S.] St Petersburg State Univ, Inst Chem, 7-9 Univ Skaya Nab, St Petersburg 199034, Russia published Easy Access to 2-Fluoro- and 2-Iodo-2H-azirines via the Halex Reaction in 2019.0, Cited 33.0. The Name is Benzyl Alcohol. Through research, I have a further understanding and discovery of 100-51-6.
A simple gram-scale method for the preparation of esters and dialkylamides of 2-(fluoro/iodo)-2H -azirine-2-carboxylic acids via the halogen exchange (Halex) reaction of 2-bromo-substituted analogues is reported. The method operates with inexpensive and safe reagents-, Bu4NF and potassium iodide, providing high product yields. Alternatively, 2-fluoro-2H-azirine-2-carboxylates can be prepared from 2-iodo- and 2-chloro-analogues. The latter compounds can be obtained in practically quantitative yield by treating the 2-iodo- and 2-bromo-2H-azirine-2-carboxylic esters with Bu4NCl.
Quality Control of Benzyl Alcohol. About Benzyl Alcohol, If you have any questions, you can contact Agafonova, AV; Smetanin, IA; Rostovskii, NV; Khlebnikov, AF; Novikov, MS or concate me.
Reference:
Indole alkaloid derivatives as building blocks of natural products from Bacillus thuringiensis and Bacillus velezensis and their antibacterial and antifungal activity study,
,Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles