244-76-8, 9H-Pyrido[2,3-b]indole is a indole-building-block compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
A round bottom flask was charged with 9H-pyrido [2,3-b] indole (3.5 g, 21 mmol)1-bromo-4-iodobenzene (8.83 g, 31 mmol), copper (I) iodide (0.8 g, 4.2 mmol),(¡À) -trans-1,2-diaminocyclohexane (0.48 g, 4.2 mmol),Potassium phosphate tribasic (8.9 g, 42 mmol) was added and dissolved in 160 ml of toluene.Was refluxed and stirred for 24 hours. Thin layer chromatography (TLC) andAfter confirming by HPLC, the reaction was terminated. After filtration, the column (MC: Hex = 1: 4)To obtain a solid compound (5.19 g, yield = 75%)., 244-76-8
The synthetic route of 244-76-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; LG Display Co., Ltd.; Choi Hye-ok; Lee Seung-jae; Pin Jong-gwan; Seo Bo-min; (39 pag.)KR2018/44695; (2018); A;,
Indole alkaloid derivatives as building blocks of natural products from?Bacillus thuringiensis?and?Bacillus velezensis?and their antibacterial and antifungal activity study
Preparation of Indole Containing Building Blocks for the Regiospecific Construction of Indole Appended Pyrazoles and Pyrroles